[Home]History of Distillation

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Revision 4 . . December 19, 2001 7:34 pm by (logged).200.130.xxx [Added explanation of separation mechanism]
Revision 3 . . (edit) August 18, 2001 12:18 am by Koyaanis Qatsi
  

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Changed: 5c5,9
The device used to effect a distillation is referred to as a still and consists, at minimum, of a pot in which the source material is heated, a condensor in which the heated vapor is cooled back to the liquid state, and a receiver in which the concentrated or purified liquid is collected.
The device used to effect a distillation is referred to as a still and consists, at minimum, of a pot in which the source material is heated, a condenser in which the heated vapor is cooled back to the liquid state, and a receiver in which the concentrated or purified liquid is collected.

The equipment may effect separation by one of two main methods. Firstly the vapours given off by the heated mixture may consist of two liquids with significantly different boiling points. Thus, the vapour that is given off is in the vast majority of one or the other liquid, which after condensation and collection effects the separation.

The second method is more effective at separating liquids with similar boiling points. This method relies upon a gradient of temperatures existing in the condenser stage of the equipment. Often in this technique, a vertical condenser , or column, is used. By extracting products that are liquid at different heights up the column, it is possible to extract liquids that have different boiling points. The greater the distance over which the temperature gradient in the condenser is applied leads to easier and greater separation.

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